Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method

CORC > 新疆理化技术研究所 > 中国科学院新疆理化技术研究所 > 中国科学院特殊环境功能材料与器件重点试验室

	Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method
	Chen, L (Chen, Long); Kong, WW (Kong, Wenwen); Yao, JC (Yao, Jincheng); Zhang, HH (Zhang, Huhnin); Gao, B (Gao, Bo); Li, YL (Li, Yonglei); Bu, HJ (Bu, Haijun); Chang, AM (Chang, Aimin); Jiang, CP (Jiang, Chunping)
刊名	CERAMICS INTERNATIONAL
	2015
卷号	41 期号:2 页码:2847-2851
关键词	Mn-Co-Ni-O nanoparticles Reverse microemulsion method Calcination temperature
ISSN号	0272-8842
通讯作者	Chang, AM
英文摘要	Mn-Co-Ni-O ultrafine ceramic nanoparticles are successfully synthesized by the reverse microemulsion method in a triton X-100/n-hexanol/cyclohexane system. The thermal decomposition process, crystallinity and crystal structure of Mn-Co-Ni-O powders are investigated and characterized by thermogravimetric-differential scanning calorimetry (TG/DSC), Fourier Transform Infrared (FT-IR), X-ray powders diffraction (XRD) and High Resolution Transmission Electron Microscope (HRTEM), respectively. The TGA/DSC, FT-IR and XRD results show that the reverse microemulsion method can effectively reduce the calcination temperature to 600 degrees C for synthesizing cubic spinel phase Mn-Co-Ni-O ceramic particles. Furthermore, the XRD and HRTEM images reveal that the particles are highly crystalline and have a narrow and uniform particle size distribution. These findings indicate that Mn-Co-Ni-O nanoparticles prepared via reverse microemulsion process meet demands for obtaining better microstructure and performance of Mn-Co-Ni-O materials.
收录类别	SCI
WOS记录号	WOS:000348003100027
公开日期	2015-03-10
内容类型	期刊论文
源URL	[http://ir.xjipc.cas.cn/handle/365002/4202]
专题	新疆理化技术研究所_中国科学院特殊环境功能材料与器件重点试验室新疆理化技术研究所_材料物理与化学研究室
作者单位	Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Funct Mat & Devices Special Environm, Key Lab Elect Informat Mat & Devices, Urumqi 830011, Xinjiang, Peoples R China;Univ Chinese Acad Sci, Beijing 100049, Peoples R China;Chinese Acad Sci, Key Lab Nanodevices & Applicat, Suzhou Inst Nanotech & Nanob, Suzhou 215123, Peoples R China
推荐引用方式 GB/T 7714	Chen, L ,Kong, WW ,Yao, JC ,et al. Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method[J]. CERAMICS INTERNATIONAL,2015,41(2):2847-2851.
APA	Chen, L .,Kong, WW .,Yao, JC .,Zhang, HH .,Gao, B .,...&Jiang, CP .(2015).Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method.CERAMICS INTERNATIONAL,41(2),2847-2851.
MLA	Chen, L ,et al."Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method".CERAMICS INTERNATIONAL 41.2(2015):2847-2851.