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Isolation and Characterization of Microcrystalline Cellulose from Distillers Grains
Ren, Haiwei2,3; Zhao, Tuo2; Xing, Junmei2; Zhang, Yi2; Li, Zhizhong2; Wang, Yonggang2; Ma, Wenpeng1
刊名JOURNAL OF BIOBASED MATERIALS AND BIOENERGY
2015-10
卷号9期号:5页码:515-522
关键词Microcrystalline Cellulose (MCC) Distillers Grains Acid Hydrolysis Structural Characterization Degree of Polymerization (DP)
ISSN号1556-6560
DOI10.1166/jbmb.2015.1550
英文摘要Although distillers grains (DG) is an inexpensive and abundant co-product that contains valuable cellulose, it is currently not being used for industrial applications. In this study, nnicrocrystalline cellulose (DGMCC) was successfully prepared from DG cellulose (DGC) using acid hydrolysis method. The effects of processing parameters like hydrochloric acid concentration, hydrolysis temperature and time on yield and degree of polymerization (DP) of DGMCC were investgated. Futhermore, DGMCC samples were characterized through various techniques, scanning electron microscopy (SEM), infrared spectroscopy (FTIR), thermogravimetry analysis (TGA) and X-ray diffraction (XRD) and compared with commercial MCC (Lowa (R) PH101). FTIR analyses demonstrated that most hemicellulose and lignin of the distillers grains fibres were removed during the extraction process. The SEM morphology shows that the DGMCC sample consisted of large round microparticles, which appear irregular but overall spherical in shape. The DGMCC was more crystalline than the native cellulose isolated from DG while maintaining the cellulose I structure. Furthermore, a good thermal stability was shown for DGMCC. Based on these analyses, DGMCC shows tremendous potential use as composites reinforcing agent, foods stabilizer and pharmaceutical additive.
资助项目National Natural Science Foundation of China[51366009] ; Natural Science Foundation of Gansu[145RJZA064][148RJZA015] ; Research & Development programs of the Gansu Education Department[2014A-030] ; Hongliu Excellent Young Teachers Cultivation Project of Lanzhou University of Technology[Q201207] ; Young teachers cultivation fund of the Xinjiang Research and Development programs[XJEDU2014S086]
WOS研究方向Chemistry ; Energy & Fuels ; Materials Science
语种英语
出版者AMER SCIENTIFIC PUBLISHERS
WOS记录号WOS:000368470200008
状态已发表
内容类型期刊论文
源URL[http://119.78.100.223/handle/2XXMBERH/33966]  
专题生命科学与工程学院
通讯作者Ren, Haiwei
作者单位1.Xinjiang Agr Vocat Tech Coll, Changji 831100, Peoples R China
2.Lanzhou Univ Technol, Sch Life Sci & Engn, Lanzhou 730050, Peoples R China
3.Lanzhou Univ Technol, China Western Res Ctr Energy & Environm, Lanzhou 730050, Peoples R China
推荐引用方式
GB/T 7714
Ren, Haiwei,Zhao, Tuo,Xing, Junmei,et al. Isolation and Characterization of Microcrystalline Cellulose from Distillers Grains[J]. JOURNAL OF BIOBASED MATERIALS AND BIOENERGY,2015,9(5):515-522.
APA Ren, Haiwei.,Zhao, Tuo.,Xing, Junmei.,Zhang, Yi.,Li, Zhizhong.,...&Ma, Wenpeng.(2015).Isolation and Characterization of Microcrystalline Cellulose from Distillers Grains.JOURNAL OF BIOBASED MATERIALS AND BIOENERGY,9(5),515-522.
MLA Ren, Haiwei,et al."Isolation and Characterization of Microcrystalline Cellulose from Distillers Grains".JOURNAL OF BIOBASED MATERIALS AND BIOENERGY 9.5(2015):515-522.
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