Preparation and characterization of YMnO3 nanoparticles

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	Preparation and characterization of YMnO3 nanoparticles
	Wang, Shifa 1,2; Yang, Hua 1,2; Xian, Tao 2; Jiang, Jinlong 2; Wei, Zhiqiang 2; Feng, Youcai 2; Li, Ruishan 2; Feng, Wangjun 2
刊名	Kuei Suan Jen Hsueh Pao/Journal of the Chinese Ceramic Society
	2010-12-01
卷号	38 期号:12 页码:2303-2307
关键词	Amides Differential scanning calorimetry Fourier transform infrared spectroscopy Gelation Magnetic materials Manganese compounds Manganites Nanomagnetics Nanoparticles Particle size Particle size analysis Scanning electron microscopy Solid state reactions Thermogravimetric analysis Calcining temperature Modified polyacrylamides Polyacrylamide gel method Solid state reaction method Structural frameworks Synthesis temperatures Thermal decomposition process Yttrium manganites
ISSN号	04545648
英文摘要	A modified polyacrylamide gel route was used to fabricate YMnO3 nanoparticles. In this route, the aqueous solution of inorganic Y and Mn salt was gelled by using acrylamide; during the gelation process, acrylamide was polymerized to form a polymer network, which provided a structural framework for the growth of particles. The X-ray diffraction, thermogravimetric analysis, differential scanning calorimetry analysis, and Fourier transform infrared spectroscopy were used in combination to investigate the thermal decomposition process of xerogel and the formation of YMnO3 phase. It is demonstrated that high-purity YMnO3 powders can be prepared at a calcining temperature of 800 °C, which is nearly 300 °C lower than the synthesis temperature based on the solid-state reaction method. The scanning electron microscopy observation reveals that the prepared YMnO3 powder has a uniform particle size, and the particles are almost spherical. The magnetic hysteresis loop measurement shows that YMnO3 nanoparticles exhibit weak ferromagnetism at room temperature, which is different from the magnetic property of bulk samples.
语种	中文
出版者	Chinese Ceramic Society
内容类型	期刊论文
源URL	[http://ir.lut.edu.cn/handle/2XXMBERH/111199]
专题	理学院省部共建有色金属先进加工与再利用国家重点实验室
作者单位	1.State Key Laboratory of Gansu Advanced Non-Ferrous Metal Materials, Lanzhou University of Technology, Lanzhou 730050, China; 2.School of Science, Lanzhou University of Technology, Lanzhou 730050, China
推荐引用方式 GB/T 7714	Wang, Shifa,Yang, Hua,Xian, Tao,et al. Preparation and characterization of YMnO3 nanoparticles[J]. Kuei Suan Jen Hsueh Pao/Journal of the Chinese Ceramic Society,2010,38(12):2303-2307.
APA	Wang, Shifa.,Yang, Hua.,Xian, Tao.,Jiang, Jinlong.,Wei, Zhiqiang.,...&Feng, Wangjun.(2010).Preparation and characterization of YMnO3 nanoparticles.Kuei Suan Jen Hsueh Pao/Journal of the Chinese Ceramic Society,38(12),2303-2307.
MLA	Wang, Shifa,et al."Preparation and characterization of YMnO3 nanoparticles".Kuei Suan Jen Hsueh Pao/Journal of the Chinese Ceramic Society 38.12(2010):2303-2307.