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Synthesis of Fe3Al-Al2O3 composite powders by mechanochemical reaction
Jia, Jian-Gang1; Guo, Tie-Ming1; Zhang, Jian-Bin1; An, Liang2; Ji, Gen-Shun1; Ma, Qin1
刊名Cailiao Rechuli Xuebao/Transactions of Materials and Heat Treatment
2013-06-01
卷号34期号:6页码:1-4
关键词Ball milling Iron oxides Milling (machining) Nanocomposites Powders Solid solutions Composite powders FeAl intermetallics Mechanical force Mechanochemical reactions Mechanochemicals Nano-composite powders Phase evolutions Structural development
ISSN号10096264
英文摘要Fe3Al-Al2O3 nano-composite powders were synthesized by mechanochemical reaction of Fe3O4-Al powder mixtures. Phase evolution and structural development during ball milling were investigated by XRD, SEM equipped with EDS. The results show that after milling for 30 min, a small quantity of Al2O3 is formed. Most of Fe3O4 is reduced by Al and α-Al2O3, θ-Al2O3, Fe(Al) solid solution and FeO are formed after milling for 1 h. After milling for 3 h, θ-Al2O3 is transformed to α-Al2O3, while Fe(Al) solid solution, FeO and the residual Al are transformed to FeAl intermetallic and Fe.911O due to the mechanical force. Continuous milling for 5 h, FeAl intermetallis reacts with Fe.911O completely and Fe3Al-Al2O3 composite powders are obtained. The mechanically activated reaction between Fe3O4 and Al is suddenly occurring type and the critical milling time is 50 min.
语种中文
出版者Editorial Office of Transactions of Materials, 18 Xueqing Road, Beijing, 100083, China
内容类型期刊论文
源URL[http://ir.lut.edu.cn/handle/2XXMBERH/113437]  
专题材料科学与工程学院
省部共建有色金属先进加工与再利用国家重点实验室
作者单位1.State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology, Lanzhou 730050, China;
2.Lanzhou Institute of Technology, Lanzhou 730050, China
推荐引用方式
GB/T 7714
Jia, Jian-Gang,Guo, Tie-Ming,Zhang, Jian-Bin,et al. Synthesis of Fe3Al-Al2O3 composite powders by mechanochemical reaction[J]. Cailiao Rechuli Xuebao/Transactions of Materials and Heat Treatment,2013,34(6):1-4.
APA Jia, Jian-Gang,Guo, Tie-Ming,Zhang, Jian-Bin,An, Liang,Ji, Gen-Shun,&Ma, Qin.(2013).Synthesis of Fe3Al-Al2O3 composite powders by mechanochemical reaction.Cailiao Rechuli Xuebao/Transactions of Materials and Heat Treatment,34(6),1-4.
MLA Jia, Jian-Gang,et al."Synthesis of Fe3Al-Al2O3 composite powders by mechanochemical reaction".Cailiao Rechuli Xuebao/Transactions of Materials and Heat Treatment 34.6(2013):1-4.
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