Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process

doi:10.1007/s11595-017-1712-9

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	Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process
	Zhu Donghai; Nai Xueying; Lan Shengjie; Dang Li; Liu Xin; Li Wu
刊名	JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION
	2017-10
卷号	32 期号:5 页码:1067-1071
ISSN号	1000-2413
DOI	10.1007/s11595-017-1712-9
英文摘要	Single crystalline calcium chloroborate (Ca2B5O9Cl) whiskers with uniform diameter have been fabricated by a two-step process. The precursor was firstly prepared by the sedimentation reaction between CaCl2, H3BO3 and NaOH aqueous solutions, and then sintered at different temperatures for 6 h with KCl as flux. The XRD indicates that the product synthesized at 600 degrees C is Orthorhombic Ca2B5O9Cl. SEM and TEM results show that the Ca2B5O9Cl is whisker with the diameter about 0.2-0.5 mu m and the length up to 15 mu m. SAED analysis shows that the whisker is single crystalline and grows along [001] direction. The possible formation process and growth mechanism were proposed.
内容类型	期刊论文
源URL	[http://ir.isl.ac.cn/handle/363002/34539]
专题	青海盐湖研究所_盐湖资源与化学实验室
推荐引用方式 GB/T 7714	Zhu Donghai,Nai Xueying,Lan Shengjie,et al. Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process[J]. JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,2017,32(5):1067-1071.
APA	Zhu Donghai,Nai Xueying,Lan Shengjie,Dang Li,Liu Xin,&Li Wu.(2017).Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process.JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,32(5),1067-1071.
MLA	Zhu Donghai,et al."Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process".JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION 32.5(2017):1067-1071.