Room temperature Mossbauer characterization of ferrites with spinel structure | |
Wang, Jing1,2; Wu, Hai-Yan1; Yang, Cai-Qin1; Lin, Yu-Long1 | |
刊名 | MATERIALS CHARACTERIZATION |
2008-12-01 | |
卷号 | 59期号:12页码:1716-1720 |
关键词 | Mossbauer spectroscopy Cobalt Gallium Doping Cation distribution |
ISSN号 | 1044-5803 |
其他题名 | Mater. Charact. |
中文摘要 | Co- and Ga-doped magnetites were synthesized at room temperature and CoFe(2)O(4) was synthesized at 60 degrees C. They were analyzed by Mossbauer analysis, X-ray diffraction, scan electron microscopy as well as magnetization determination. The information of composition, cation distribution in the spinel structure and the particle size distribution of the products were obtained. Meanwhile, the formation mechanism of Co-doped magnetite was deduced. Two different procedures were used to precipitate CoFe(2)O(4) magnetic particles. One was named normal pH regulation procedure (A) in which alkaline solution was dropped into the mixture solution of metal ions and the other was denoted as reverse pH regulation procedure (B) in which mixture solution of metal ions were dropped into alkaline solution. Particles of uniform size were obtained in procedure A, which resulted from calculated average particle size and Mossbauer analysis. A comparative original method for investigating the magnetic nanoparticle size distribution was developed. (C) 2008 Elsevier Inc. All rights reserved. |
英文摘要 | Co- and Ga-doped magnetites were synthesized at room temperature and CoFe(2)O(4) was synthesized at 60 degrees C. They were analyzed by Mossbauer analysis, X-ray diffraction, scan electron microscopy as well as magnetization determination. The information of composition, cation distribution in the spinel structure and the particle size distribution of the products were obtained. Meanwhile, the formation mechanism of Co-doped magnetite was deduced. Two different procedures were used to precipitate CoFe(2)O(4) magnetic particles. One was named normal pH regulation procedure (A) in which alkaline solution was dropped into the mixture solution of metal ions and the other was denoted as reverse pH regulation procedure (B) in which mixture solution of metal ions were dropped into alkaline solution. Particles of uniform size were obtained in procedure A, which resulted from calculated average particle size and Mossbauer analysis. A comparative original method for investigating the magnetic nanoparticle size distribution was developed. (C) 2008 Elsevier Inc. All rights reserved. |
WOS标题词 | Science & Technology ; Technology |
类目[WOS] | Materials Science, Characterization & Testing |
研究领域[WOS] | Materials Science |
关键词[WOS] | MAGNETIC-PROPERTIES ; CATION DISTRIBUTION ; IRON-OXIDE ; MECHANISM |
收录类别 | SCI |
原文出处 | |
语种 | 英语 |
WOS记录号 | WOS:000262071500006 |
公开日期 | 2013-10-08 |
内容类型 | 期刊论文 |
版本 | 出版稿 |
源URL | [http://ir.ipe.ac.cn/handle/122111/2861] |
专题 | 过程工程研究所_研究所(批量导入) |
作者单位 | 1.Hebei Med Univ, Sch Pharmaceut Sci, Shijiazhuang 050017, Peoples R China 2.Chinese Acad Sci, Inst Proc Engn, Beijing 100081, Peoples R China |
推荐引用方式 GB/T 7714 | Wang, Jing,Wu, Hai-Yan,Yang, Cai-Qin,et al. Room temperature Mossbauer characterization of ferrites with spinel structure[J]. MATERIALS CHARACTERIZATION,2008,59(12):1716-1720. |
APA | Wang, Jing,Wu, Hai-Yan,Yang, Cai-Qin,&Lin, Yu-Long.(2008).Room temperature Mossbauer characterization of ferrites with spinel structure.MATERIALS CHARACTERIZATION,59(12),1716-1720. |
MLA | Wang, Jing,et al."Room temperature Mossbauer characterization of ferrites with spinel structure".MATERIALS CHARACTERIZATION 59.12(2008):1716-1720. |
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