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Synthesis of CoFe2O4 nanoparticles with tunable magnetism by the modified hydrothermal method
Zhang, Yue1,2; Liu, Yong1,2; Yang, Zhi1,2; Xiong, Rui1,2,3; Shi, Jing1,2,3,4
刊名JOURNAL OF NANOPARTICLE RESEARCH
2011-10-01
卷号13期号:10页码:4557-4563
关键词Cobalt ferrite Nanoparticles Hydrothermal method Magnetism
ISSN号1388-0764
DOI10.1007/s11051-011-0412-1
通讯作者Xiong, Rui(xiongrui1967@163.com)
英文摘要Cobalt ferrite (CoFe2O4) nanoparticles were synthesized by using the hydrothermal route with the addition of trisodium citrate dihydrate (Na(3)CA center dot 2H(2)O). The formation of CoFe2O4 nanoparticles with size ranging from 13 to 19 nm was confirmed by X-ray diffraction, energy dispersive X-ray analysis, and Fourier transform infrared spectroscopy; the clear-cut sharp of the nanoparticles was observed by transmission electron microscopy. By these characterization methods, the evolution of lattice constant and morphologies of the nanoparticles with the addition of Na(3)CA center dot 2H(2)O is observed. Furthermore, the magnetic hysteresis loops measured at room temperature indicate that the magnetic properties of the products also show clear relationship with the masses of Na(3)CA center dot 2H(2)O. For example, coercivity and high-field paramagnetic susceptibility increase with the increasing masses of Na(3)CA center dot 2H(2)O, whereas the saturation magnetization and the effective magnetic anisotropy constant have the maximum values as the mass of Na(3)CA center dot 2H(2)O is 1 g. This change of magnetic properties is related with the expanded lattice and the varied size and shape because of the addition of Na(3)CA center dot 2H(2)O.
资助项目Chinese National Foundation of Natural Science[10974148] ; National Science Fund for Talent Training in Basic Science[J0830310] ; 973 Program[2009CB939705] ; Wuhan University[5082003]
WOS研究方向Chemistry ; Science & Technology - Other Topics ; Materials Science
语种英语
出版者SPRINGER
WOS记录号WOS:000295609700015
资助机构Chinese National Foundation of Natural Science ; National Science Fund for Talent Training in Basic Science ; 973 Program ; Wuhan University
内容类型期刊论文
源URL[http://ir.imr.ac.cn/handle/321006/104082]  
专题金属研究所_中国科学院金属研究所
通讯作者Xiong, Rui
作者单位1.Wuhan Univ, Sch Phys & Technol, Wuhan 430072, Peoples R China
2.Wuhan Univ, Key Lab Artificial Micro & Nanostruct, Minist Educ, Wuhan 430072, Peoples R China
3.Hubei Univ, Key Lab Green Preparat & Applicat Funct Mat, Minist Educ, Wuhan 430062, Peoples R China
4.Acad Sinica, Int Ctr Mat Phys, Shenyang 110015, Peoples R China
推荐引用方式
GB/T 7714
Zhang, Yue,Liu, Yong,Yang, Zhi,et al. Synthesis of CoFe2O4 nanoparticles with tunable magnetism by the modified hydrothermal method[J]. JOURNAL OF NANOPARTICLE RESEARCH,2011,13(10):4557-4563.
APA Zhang, Yue,Liu, Yong,Yang, Zhi,Xiong, Rui,&Shi, Jing.(2011).Synthesis of CoFe2O4 nanoparticles with tunable magnetism by the modified hydrothermal method.JOURNAL OF NANOPARTICLE RESEARCH,13(10),4557-4563.
MLA Zhang, Yue,et al."Synthesis of CoFe2O4 nanoparticles with tunable magnetism by the modified hydrothermal method".JOURNAL OF NANOPARTICLE RESEARCH 13.10(2011):4557-4563.
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