Simultaneous enrichment/determination of six sulfonamides in animal husbandry products and environmental waters by pressure-assisted electrokinetic injection coupled with capillary zone electrophoresis

doi:10.1016/j.jfca.2020.103462

CORC > 烟台海岸带研究所 > 中国科学院烟台海岸带研究所 > 山东省海岸带环境工程技术研究中心

	Simultaneous enrichment/determination of six sulfonamides in animal husbandry products and environmental waters by pressure-assisted electrokinetic injection coupled with capillary zone electrophoresis
	Yang, Shixuan ; Ma, Suya ; Zhu, Kongli ; Wang, Minglin ; Li, Jinhua ; Arabi, Maryam ; Liu, Huitao ; Li, Yin ; Chen, Lingxin
刊名	JOURNAL OF FOOD COMPOSITION AND ANALYSIS
	2020-05
卷号	88 页码:103462
关键词	SOLID-PHASE EXTRACTION MASS-SPECTROMETRY RESIDUES SAMPLES MILK MEAT ANTIBIOTICS METHODOLOGY STACKING URINE
DOI	10.1016/j.jfca.2020.103462
产权排序	[Yang, Shixuan ; Wang, Minglin] Shandong Agr Univ, Coll Food Sci & Engn, Tai An 271018, Shandong, Peoples R China ; [Yang, Shixuan ; Ma, Suya ; Li, Jinhua ; Arabi, Maryam ; Chen, Lingxin] Chinese Acad Sci, Yantai Inst Coastal Zone Res, CAS Key Lab Coastal Environm Proc & Ecol Remediat, Res Ctr Coastal Environm Engn & Technol, Yantai 264003, Peoples R China ; [Zhu, Kongli] Inspect & Testing Ctr Yinan Cty, Yinan 276300, Shandong, Peoples R China ; [Liu, Huitao] Yantai Univ, Coll Chem & Chem Engn, Yantai 264005, Peoples R China ; [Li, Yin] Naval Aviat Univ, Yantai 264001, Peoples R China
文献子类	Article
英文摘要	Pressure-assisted electrokinetic injection (PAEKI) as the online method was developed for the simultaneous enrichment of six sulfonamides (SAs), including sulfamethazine (SMZ), sulfamerazine (SMR), sulfamono-methoxine (SMM), sulfadizine (SDZ), sulfamethoxazole (SMX) and sulfacetamide (SFA) in different animal husbandry products and environmental waters samples, followed by capillary zone electrophoresis (CZE) determination. Various parameters affecting the separation performance of CZE and the enrichment efficiency of PAEKI were optimized in detail. Under optimal conditions, the six SAs were completely separated within 8.5 min, and the enrichment factors for SMZ, SMR, SMM, SDZ, SMX and SFA were 39, 47, 53, 50, 54 and 62 folds, respectively, compared with the direct CZE. The limits of detection (LOD) ranged from 0.0018-0.0163 mu g/mL, 0.0083-0.0638 mu g/mL and 0.0052-0.0478 mu g/mL in milk, pork and egg samples, respectively, as well as limits of quantification (LOQ) within 0.0061-0.0503 mu g/mL, 0.0253-0.1826 mu g/mL and 0.0164-0.1475 mu g/mL, respectively. Tap water, lake water and seawater were also examined for investigation of applicability of the proposed method. Satisfactory recoveries in the range of 89-113 % were obtained with the three spiked food samples, and the relative standard deviations were from 1.6 to 7.3%. Simple and effective online enrichment method provides a promising perspective for CZE measurements of SAs in complex matrices with high accuracy, sensitivity and rapidity.
WOS关键词	SOLID-PHASE EXTRACTION ; MASS-SPECTROMETRY ; RESIDUES ; SAMPLES ; MILK ; MEAT ; ANTIBIOTICS ; METHODOLOGY ; STACKING ; URINE
语种	英语
WOS记录号	WOS:000525346100025
资助机构	National Natural Science Foundation of ChinaNational Natural Science Foundation of China [21876199] ; 13th Five-Year Plan for National Key Research and Development Projects [2017YFF0211304] ; Chinese Academy of Sciences President's International Fellowship Initiative [2019PC0050] ; Taishan Scholar Project Special Funding [ts20190962]
内容类型	期刊论文
源URL	[http://ir.yic.ac.cn/handle/133337/25040]
专题	烟台海岸带研究所_山东省海岸带环境工程技术研究中心烟台海岸带研究所_中科院海岸带环境过程与生态修复重点实验室
作者单位	1.Chinese Acad Sci, Yantai Inst Coastal Zone Res, CAS Key Lab Coastal Environm Proc & Ecol Remediat, Res Ctr Coastal Environm Engn & Technol, Yantai 264003, Peoples R China; 2.Naval Aviat Univ, Yantai 264001, Peoples R China 3.Yantai Univ, Coll Chem & Chem Engn, Yantai 264005, Peoples R China; 4.Inspect & Testing Ctr Yinan Cty, Yinan 276300, Shandong, Peoples R China; 5.Shandong Agr Univ, Coll Food Sci & Engn, Tai An 271018, Shandong, Peoples R China;
推荐引用方式 GB/T 7714	Yang, Shixuan,Ma, Suya,Zhu, Kongli,et al. Simultaneous enrichment/determination of six sulfonamides in animal husbandry products and environmental waters by pressure-assisted electrokinetic injection coupled with capillary zone electrophoresis[J]. JOURNAL OF FOOD COMPOSITION AND ANALYSIS,2020,88:103462.
APA	Yang, Shixuan.,Ma, Suya.,Zhu, Kongli.,Wang, Minglin.,Li, Jinhua.,...&Chen, Lingxin.(2020).Simultaneous enrichment/determination of six sulfonamides in animal husbandry products and environmental waters by pressure-assisted electrokinetic injection coupled with capillary zone electrophoresis.JOURNAL OF FOOD COMPOSITION AND ANALYSIS,88,103462.
MLA	Yang, Shixuan,et al."Simultaneous enrichment/determination of six sulfonamides in animal husbandry products and environmental waters by pressure-assisted electrokinetic injection coupled with capillary zone electrophoresis".JOURNAL OF FOOD COMPOSITION AND ANALYSIS 88(2020):103462.