Enhanced extraction of patchouli alcohol from Pogostemon cablin by microwave radiation-accelerated ionic liquid pretreatment
Fan L(范玲); Jin RH(靳荣华)
刊名J. Chromatogr. B
2011
卷号879页码:3653-3657
关键词Microwave radiation-accelerated ionic liquid pretreatment Ionic liquid Pogostemon cablin Patchouli alcohol Gas chromatography
ISSN号1570-0232
通讯作者陈士
中文摘要A microwave radiation-accelerated ionic liquid pretreatment (MRAILP) was developed to enhance extraction of patchouli alcohol from Pogostemon cablin. 1-N-butyl-3-methylimidazolium chloride ([C4mim]Cl) was selected as microwave absorbing and cellulose dissolution medium and microwave was applied to accelerate sample dissolution. The conditions of MRAILP including particle size, solvent, microwave pretreatment time and power and the ratio of ionic liquid (IL) to sample were optimized. Under the optimized conditions, the extraction yield of patchouli alcohol by the MRAILP was 1.94%, which has increased by 166% compared with microwave-assisted extraction. The recovery was in the range of 95.71–103.7% with relative standard deviation lower than 3.0%. It was a novel alternative extraction method for the fast extraction and determination of patchouli alcohol from Pogostemon cablin.
学科主题物理化学
收录类别SCI
资助信息the Foundation of Key Laboratory of Ecological Agriculture of Ministry of Agriculture (2009k01);President Fund of South China Agricultural University (4009k06366)
语种英语
WOS记录号WOS:000297396200041
公开日期2012-09-20
内容类型期刊论文
源URL[http://210.77.64.217/handle/362003/383]  
专题兰州化学物理研究所_OSSO国家重点实验室
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Fan L,Jin RH. Enhanced extraction of patchouli alcohol from Pogostemon cablin by microwave radiation-accelerated ionic liquid pretreatment[J]. J. Chromatogr. B,2011,879:3653-3657.
APA 范玲,&靳荣华.(2011).Enhanced extraction of patchouli alcohol from Pogostemon cablin by microwave radiation-accelerated ionic liquid pretreatment.J. Chromatogr. B,879,3653-3657.
MLA 范玲,et al."Enhanced extraction of patchouli alcohol from Pogostemon cablin by microwave radiation-accelerated ionic liquid pretreatment".J. Chromatogr. B 879(2011):3653-3657.
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