Pressure Determination by Raman Spectra of Water in Hydrothermal Diamond-Anvil Cell Experiments | |
Yang, Yuping ; Zheng, Haifei | |
刊名 | 应用光谱学 |
2009 | |
关键词 | Water Raman spectroscopy Pressure determination Diamond-anvil cells LIQUID WATER TEMPERATURE-DEPENDENCE SUPERCRITICAL FLUIDS LOW-FREQUENCY SPECTROSCOPY DYNAMICS MODEL SENSOR 500-DEGREES-C FLUORESCENCE |
DOI | 10.1366/000370209787169678 |
英文摘要 | The technique of using spectroscopic pressure gauges provides an efficient method for in-situ pressure determination in hydrothermal diamond-anvil cell (HDAC) experiments. Rhenium with a thickness of 0.33 mm was used as a gasket and the sample chamber was 0.5 mm in diameter. Pure water was loaded into the chamber of the HDAC together with a single crystal of quartz and cubic boron nitride. The experimental pressure was estimated according to the Raman shift of the 464 cm-1 peak of quartz. The sample was heated by two small furnaces made of NiFe alloy wires and the temperature was measured by a thermocouple, which was calibrated using the melting points of 1-naphthol, salicylic acid, hippuric acid and phenolphthalein at atmospheric pressure before the experiment. It was observed that the shapes of the OH stretching band of water at a certain temperature do not show variation with increasing pressure.; Instruments & Instrumentation; Spectroscopy; SCI(E); EI; PubMed; 3; ARTICLE; 1; 120-123; 63 |
语种 | 英语 |
内容类型 | 期刊论文 |
源URL | [http://ir.pku.edu.cn/handle/20.500.11897/310882] |
专题 | 地球与空间科学学院 |
推荐引用方式 GB/T 7714 | Yang, Yuping,Zheng, Haifei. Pressure Determination by Raman Spectra of Water in Hydrothermal Diamond-Anvil Cell Experiments[J]. 应用光谱学,2009. |
APA | Yang, Yuping,&Zheng, Haifei.(2009).Pressure Determination by Raman Spectra of Water in Hydrothermal Diamond-Anvil Cell Experiments.应用光谱学. |
MLA | Yang, Yuping,et al."Pressure Determination by Raman Spectra of Water in Hydrothermal Diamond-Anvil Cell Experiments".应用光谱学 (2009). |
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