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	Multiresidue determination of sulfonamides, macrolides, trimethprim, and chloramphenicol in sewage sludge and sediment using ultrasonic extraction coupled with solid phase extraction and liquid chromatography-tandem mass spectrometry
	Tang Cai-Ming1,2; Huang Qiu-Xin1,2; Yu Yi-Yi1,2; Peng Xian-Zhi1
刊名	Chinese journal of analytical chemistry
	2009-08-01
卷号	37期号:8页码:1119-1124
关键词	Ultrasonic extraction Liquid chromatography-tandem mass spectrometry Antibiotics Sewage sludge
ISSN号	0253-3820
通讯作者	Peng xian-zhi(pengx@gig.ac.cn)
英文摘要	A sensitive and feasible method was developed for the simultaneous determination of 10 trace antibiotic residues including sulfonamides, macrolides, trimethoprim and chloramphenicol in sewage sludge and sediment. the method involved ultrasonic extraction followed by solid phase extraction cleanup and liquid chromatography-tandem mass spectrometry coupled with electrospray ionization in positive mode (esi +). liquid chromatography separations were carried out by c(18) reversed phase column with the mobile phase of aqueous solution of 0.1% formic acid and 5 mmol/l ammonium acetate and methanol. the antibiotics were identified and determined by internal standard method in selected multiple reaction monitoring mode. the method detected limits were in the range from 2.2 ng/g to 66.9 ng/g dry weight for the investigated antibiotic compounds in sewage sludge. the recoveries ranged from 74.7% to 111.8% with the relative standard deviations of 1.2%-10.6%. the method was successfully applied in a primary investigation of the occurrence of antibiotic residues in-sewage sludge and a river sediment sample collected from guangzhou. sulfamethazine, trimethoprim, azithromycin, clarithromycin, dehydrated erythromycin and roxithromycin were detected in both the sewage sludge and the river sediment, ranging from 6.8-125.6 ng/g dry weight.
WOS关键词	ANTIBIOTICS ; PHARMACEUTICALS ; WASTEWATERS ; RESIDUES ; WATER ; MILK
WOS研究方向	Chemistry
WOS类目	Chemistry, Analytical
语种	英语
出版者	ELSEVIER SCIENCE INC
WOS记录号	WOS:000269596400005
内容类型	期刊论文
URI标识	http://www.corc.org.cn/handle/1471x/2395108
专题	中国科学院大学
通讯作者	Peng Xian-Zhi
作者单位	1.Chinese Acad Sci, Guangzhou Inst Geochem, State Key Lab Organ Geochem, Guangzhou 510640, Peoples R China 2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China
推荐引用方式 GB/T 7714	Tang Cai-Ming,Huang Qiu-Xin,Yu Yi-Yi,et al. Multiresidue determination of sulfonamides, macrolides, trimethprim, and chloramphenicol in sewage sludge and sediment using ultrasonic extraction coupled with solid phase extraction and liquid chromatography-tandem mass spectrometry[J]. Chinese journal of analytical chemistry,2009,37(8):1119-1124.
APA	Tang Cai-Ming,Huang Qiu-Xin,Yu Yi-Yi,&Peng Xian-Zhi.(2009).Multiresidue determination of sulfonamides, macrolides, trimethprim, and chloramphenicol in sewage sludge and sediment using ultrasonic extraction coupled with solid phase extraction and liquid chromatography-tandem mass spectrometry.Chinese journal of analytical chemistry,37(8),1119-1124.
MLA	Tang Cai-Ming,et al."Multiresidue determination of sulfonamides, macrolides, trimethprim, and chloramphenicol in sewage sludge and sediment using ultrasonic extraction coupled with solid phase extraction and liquid chromatography-tandem mass spectrometry".Chinese journal of analytical chemistry 37.8(2009):1119-1124.

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