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Surfactant-assisted synthesis and characterization of novel chain-like coni alloy assemblies
Zhu, Lu-Ping; Xiao, Hong-Mei; Fu, Shao-Yun
刊名European journal of inorganic chemistry
2007-09-01
期号25页码:3947-3951
关键词Alloy Assemblies Hydrothermal method Ferromagnetism Coercivity
ISSN号1434-1948
DOI10.1002/ejic.200700558
通讯作者Fu, shao-yun(syfu@mail.ipc.ac.cn)
英文摘要Novel chain-like coni alloy assemblies with a length of up to 6-7 inn were successfully prepared by a surfactant-assisted hydrothermal synthetic route at 100 degrees c for 2 h. the individual submicrospheres built from smaller coni nanoparticles had a diameter of about 400-500 nm. these microspheres were then integrated to form the novel chain-like coni alloy assemblies. the effects of synthetic parameters such as surfactant and solvent on the formation and morphology of coni samples were investigated. the experimental results showed that n2h4 center dot h2o and cta(+) play important roles in the formation of the novel chain-like coni alloy assemblies. based on the structural information provided by x-ray powder diffraction, scanning electron microscopy, transmission electron microscopy, selected-area electron diffraction and energydispersive x-ray analysis, a growth mechanism was tentatively proposed for the formation of chain-like coni alloy assemblies. magnetic hysteresis measurement revealed that the chain-like coni alloy assemblies display ferromagnetic behavior with a saturation magnetization of 96.15 emu/g and a coercivity of 144.75 oe at room temperature.
WOS关键词ONE-DIMENSIONAL ASSEMBLIES ; MAGNETIC-PROPERTIES ; COBALT ALLOYS ; NANOPARTICLES ; NANOWIRES ; ELECTRODEPOSITION ; NANOSTRUCTURES ; FABRICATION ; FILMS ; COPT
WOS研究方向Chemistry
WOS类目Chemistry, Inorganic & Nuclear
语种英语
出版者WILEY-V C H VERLAG GMBH
WOS记录号WOS:000249362800003
内容类型期刊论文
URI标识http://www.corc.org.cn/handle/1471x/2380109
专题中国科学院大学
通讯作者Fu, Shao-Yun
作者单位1.Chinese Acad Sci, Tech Inst Phys & Chem, Beijing 100080, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
推荐引用方式
GB/T 7714
Zhu, Lu-Ping,Xiao, Hong-Mei,Fu, Shao-Yun. Surfactant-assisted synthesis and characterization of novel chain-like coni alloy assemblies[J]. European journal of inorganic chemistry,2007(25):3947-3951.
APA Zhu, Lu-Ping,Xiao, Hong-Mei,&Fu, Shao-Yun.(2007).Surfactant-assisted synthesis and characterization of novel chain-like coni alloy assemblies.European journal of inorganic chemistry(25),3947-3951.
MLA Zhu, Lu-Ping,et al."Surfactant-assisted synthesis and characterization of novel chain-like coni alloy assemblies".European journal of inorganic chemistry .25(2007):3947-3951.
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