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Structure-controlled solventless thermolytic synthesis of uniform silver nanodisks
Chen, YB; Chen, L; Wu, LM
刊名Inorganic chemistry
2005-12-26
卷号44期号:26页码:9817-9822
ISSN号0020-1669
DOI10.1021/ic051246d
通讯作者Wu, lm()
英文摘要Monodisperse silver nanodisks are synthesized on the gram scale from a well-characterized layered silver thiolate precursor via thermolysis at 180-225 degrees c under a n-2 atmosphere. xrd, tem, hrtem, and afm analyses indicate that the nanodisks generated at 180 degrees c over 2 h have an average diameter of about 16.1 nm (sigma = +/- 12%) and a thickness of 2.3 nm (sigma = +/- 14%), and they lie on their (111) faces. the disk shape is considered to be predestined by the crystal structure of the precursor. important aspects regarding the stability of the precursor, the thermolysis temperature, and the annealing time, as well as a possible conversion mechanism, are discussed.
WOS关键词SEMICONDUCTOR NANOWIRES ; LAYERED STRUCTURE ; SULFIDE NANORODS ; ASPECT RATIO ; GROWTH ; GOLD ; TEMPLATES
WOS研究方向Chemistry
WOS类目Chemistry, Inorganic & Nuclear
语种英语
出版者AMER CHEMICAL SOC
WOS记录号WOS:000234192300035
内容类型期刊论文
URI标识http://www.corc.org.cn/handle/1471x/2377604
专题中国科学院大学
通讯作者Wu, LM
作者单位1.Chinese Acad Sci, Fujian Inst Res Struct Matter, State Key Lab Struct Chem, Fujian 350002, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
推荐引用方式
GB/T 7714
Chen, YB,Chen, L,Wu, LM. Structure-controlled solventless thermolytic synthesis of uniform silver nanodisks[J]. Inorganic chemistry,2005,44(26):9817-9822.
APA Chen, YB,Chen, L,&Wu, LM.(2005).Structure-controlled solventless thermolytic synthesis of uniform silver nanodisks.Inorganic chemistry,44(26),9817-9822.
MLA Chen, YB,et al."Structure-controlled solventless thermolytic synthesis of uniform silver nanodisks".Inorganic chemistry 44.26(2005):9817-9822.
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