Sol concentration effect on ZnO nanofibers photocatalytic activity synthesized by sol-gel dip coating method
Toubane, M.1,2; Tala-Ighil, R.2,3; Bensouici, F.1,2; Bououdina, M.4; Souier, M.5; Liu, S.6; Cai, W.6; Iratni, A.2
刊名MATERIALS RESEARCH EXPRESS
2017-03-01
卷号4期号:3页码:1-17
关键词Dip Coating Sol Concentration Fesem Afm Photocatalysis Zno Nanofibers
DOI10.1088/2053-1591/aa61cf
文献子类Article
英文摘要ZnO thin films were deposited onto glass substrate by sol-gel dip coating method. The initial sol concentrations were varied from 0.2 to 0.5 M. Zinc acetate dihydrate, ethanol and Diethanolamine (DEA) were used as staring material, solvent and stabilizer respectively. The evolution of structural, optical properties and methylene blue (MB) photodegradation of the as-deposited films on sol concentration was investigated. Rietveld refinements of x-ray patterns reveal that all the as-prepared thin films have a Zincite-type structure with grain orientation along to c-axis. The strongest sol concentration is favorable for the highest crystallization quality. However, the high preferred orientation factor (POF) occurs for 0.3 M sol concentration. The field emission scanning electron microscopy observations reveals nanofibrous morphology with different lengths. The nanofibers density increases with increasing sols concentrations until forming a flower-like morphology. The EDS analysis confirms the high purity of the as-deposited ZnO films. It is found that all films present good transparency greater than 95% in the visible range; the optical band gap is slightly reduced with the increase in sol concentration. The photocatalytic degradation is enhanced by 90% with the sol concentration. The K-app rate reaction increased with increasing sol concentration. The films stability is found to slightly decrease after the third cycle, especially for 0.5 M sol concentration.
WOS关键词POWER SPECTRAL DENSITY ; THIN-FILMS ; OPTICAL-PROPERTIES ; SPRAY-PYROLYSIS ; VISIBLE-LIGHT ; PHOTODEGRADATION KINETICS ; ANNEALING TEMPERATURE ; TITANIUM-DIOXIDE ; DEGRADATION ; TIO2
WOS研究方向Materials Science
语种英语
WOS记录号WOS:000398787000004
资助机构Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016) ; Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016) ; Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016) ; Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016) ; Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016) ; Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016) ; Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016) ; Chinese Academy of Science (CAS) through CAS president's International Fellowship Initiative(2015 VTA016)
内容类型期刊论文
源URL[http://ir.hfcas.ac.cn:8080/handle/334002/32959]  
专题合肥物质科学研究院_中科院固体物理研究所
作者单位1.Mhammed Bougara Univ, Dept Phys, Fac Sci, Boumerdes 35000, Algeria
2.Mhammed Bougara Univ, URMPE Unit, Boumerdes 35000, Algeria
3.Mhammed Bougara Univ, Inst Elect & Elect Engn, Boumerdes 35000, Algeria
4.Univ Bahrain, Coll Sci, Dept Phys, POB 32038, Sakheer, Bahrain
5.Sultan Qaboos Univ, Coll Sci, Dept Phys, POB 36, Muscat, Oman
6.Chinese Acad Sci, Inst Solid State Phys, Ctr Environm & Energy Nanomat, Anhui Key Lab Nanomat & Nanotechnol,Key Lab Mat P, Hefei 230031, Peoples R China
推荐引用方式
GB/T 7714
Toubane, M.,Tala-Ighil, R.,Bensouici, F.,et al. Sol concentration effect on ZnO nanofibers photocatalytic activity synthesized by sol-gel dip coating method[J]. MATERIALS RESEARCH EXPRESS,2017,4(3):1-17.
APA Toubane, M..,Tala-Ighil, R..,Bensouici, F..,Bououdina, M..,Souier, M..,...&Iratni, A..(2017).Sol concentration effect on ZnO nanofibers photocatalytic activity synthesized by sol-gel dip coating method.MATERIALS RESEARCH EXPRESS,4(3),1-17.
MLA Toubane, M.,et al."Sol concentration effect on ZnO nanofibers photocatalytic activity synthesized by sol-gel dip coating method".MATERIALS RESEARCH EXPRESS 4.3(2017):1-17.
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