Nitrate-citrate combustion synthesis and properties of Ce1-xSmxO2-x/2 solid solutions | |
Peng, C. ; Zhang, Y. ; Cheng, Z. W. ; Cheng, X. ; Meng, J. ; Zhang Y(张颖) | |
刊名 | http://dx.doi.org/10.1023/A:1021556431397 |
2002-12 | |
关键词 | ELECTRICAL-PROPERTIES X-RAY ELECTROLYTES PEROVSKITE CELL |
英文摘要 | A nitrate-citrate combustion route to synthesize nanocrystalline samarium-doped ceria powders for solid electrolyte ceramics is presented. This route is based on the gelling of nitrate solutions by the addition of citric acid and ammonium hydroxide, followed by an intense combustion process due to an exothermic redox reaction between nitrate and citrate ions. The influence of ignition temperature on the characteristics of the powders was studied. The change of the crystal structure with the content of doped Sm was investigated. High temperature X-ray, and Raman scattering were used to characterize the sample. The lattice constant and unit volume increase with doping level and increasing temperature. Dense ceramic samples prepared by uniaxial pressing and sintering in air were also studied. (C) 2002 Kluwer Academic Publishers. |
语种 | 英语 |
内容类型 | 期刊论文 |
源URL | [http://dspace.xmu.edu.cn/handle/2288/59347] |
专题 | 材料学院-已发表论文 |
推荐引用方式 GB/T 7714 | Peng, C.,Zhang, Y.,Cheng, Z. W.,et al. Nitrate-citrate combustion synthesis and properties of Ce1-xSmxO2-x/2 solid solutions[J]. http://dx.doi.org/10.1023/A:1021556431397,2002. |
APA | Peng, C.,Zhang, Y.,Cheng, Z. W.,Cheng, X.,Meng, J.,&张颖.(2002).Nitrate-citrate combustion synthesis and properties of Ce1-xSmxO2-x/2 solid solutions.http://dx.doi.org/10.1023/A:1021556431397. |
MLA | Peng, C.,et al."Nitrate-citrate combustion synthesis and properties of Ce1-xSmxO2-x/2 solid solutions".http://dx.doi.org/10.1023/A:1021556431397 (2002). |
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