Quantitative convergent-beam electron diffraction: II. Application in La/sub 2/3/Ca/sub 1/3/MnO/sub 3/ | |
Feng Fang ; Zhang Ai-hua ; Zhu Jing | |
2010-05-10 ; 2010-05-10 | |
关键词 | Experimental/ calcium compounds crystal symmetry Debye-Waller factors electron diffraction lanthanum compounds/ quantitative convergent-beam electron diffraction symmetry operation image distortion correction multistart clustering global optimization algorithm atomic position parameters temperature factors Debye-Waller factors Laue zone energy-filtered diffraction patterns La/sub 0.67/Ca/sub 0.33/MnO/sub 3// A6160 Crystal structure of specific inorganic compounds A6150E Crystal symmetry models and space groups, and crystalline systems and classes A6370 Statistical mechanics of lattice vibrations/ La0.67Ca0.33MnO3/ss Ca0.33/ss La0.67/ss O3/ss Ca/ss La/ss Mn/ss O/ss |
中文摘要 | Quantitative convergent-beam electron diffraction method (QCBED) was applied to study the complex oxide, La/sub 2/3/Ca/sub 1/3/MnO/sub 3/. For this purpose, some modifications, including the consideration of symmetry operation, the image distortion correction and multi-start clustering global optimization algorithm, to the QCBED experiments and optimization program were explored according to the structure feature of La/sub 2/3/Ca/sub 1/3/MnO/sub 3/. The way to refine atomic position parameters and temperature factors (Debye-Waller factors) without an energy-filter is attempted with the diffraction intensity of high-order Laue zone. Based on these refined atomic position parameters and temperature factors, the nine structure factors of the low-index diffractions were refined by fitting the energy-filtered diffraction patterns with the improved QCBED method. |
语种 | 中文 ; 中文 |
出版者 | Chinese Electron Microscopy Society ; China |
内容类型 | 期刊论文 |
源URL | [http://hdl.handle.net/123456789/20421] |
专题 | 清华大学 |
推荐引用方式 GB/T 7714 | Feng Fang,Zhang Ai-hua,Zhu Jing. Quantitative convergent-beam electron diffraction: II. Application in La/sub 2/3/Ca/sub 1/3/MnO/sub 3/[J],2010, 2010. |
APA | Feng Fang,Zhang Ai-hua,&Zhu Jing.(2010).Quantitative convergent-beam electron diffraction: II. Application in La/sub 2/3/Ca/sub 1/3/MnO/sub 3/.. |
MLA | Feng Fang,et al."Quantitative convergent-beam electron diffraction: II. Application in La/sub 2/3/Ca/sub 1/3/MnO/sub 3/".(2010). |
个性服务 |
查看访问统计 |
相关权益政策 |
暂无数据 |
收藏/分享 |
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。
修改评论