Preparation of Hydroxyapatite-titanium Dioxide Coating on Ti6Al4V Substrates using Hydrothermal-electrochemical Method
He Daihua1; Wang Pu2; Liu Ping1; Liu Xinkuan1; Ma Fengcang1; Li Wei1; Chen Xiaohong1; Zhao Jun3; Ye Hong4
刊名JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION
2016-04-01
卷号31期号:2页码:461-467
关键词Ti6Al4V HA-TiO2 coating anodic oxidation hydrothermal-electrochemical method
英文摘要Ti6Al4V substrates were anodized in a 0.5 mol/L H2SO4 solution at applied voltages of 90-140 V. A hydroxyapatite-titanium oxide (HA-TiO2) coating was then deposited on the anodized Ti6Al4V substrates via a hydrothermal-electrochemical method at a constant current. The obtained films and coatings were characterized by X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and Fourier-transform infrared spectrometry. The microstructures of the porous films on the Ti6Al4V substrates were studied to investigate the effect of the anodizing voltage on the phase and morphology of the HA-TiO2 coating. The results indicated that both the phase composition and the morphology of the coatings were significantly influenced by changes in the anodizing voltage. HA-TiO2 was directly precipitated onto the surface of the substrate when the applied voltage was between 110 and 140 V. The coatings had a gradient structure and the HA exhibited both needle-like and cotton-like structures. The amount of cotton-like HA structures decreased with an increase in voltage from 90 to 120 V, and then increased slightly when the voltage was higher than 120 V. The orientation index of the (002) plane of the coating was at a minimum when the Ti6Al4V substrate was pretreated at 120 V.
WOS标题词Science & Technology ; Technology
类目[WOS]Materials Science, Multidisciplinary
研究领域[WOS]Materials Science
关键词[WOS]MICRO-ARC OXIDATION ; CALCIUM-PHOSPHATE ; ANODIC-OXIDATION ; ALKALI TREATMENT ; DEPOSITION ; ALLOY ; NANOCRYSTALS ; GROWTH ; FILM
收录类别SCI
语种英语
WOS记录号WOS:000377017600036
内容类型期刊论文
源URL[http://ir.sic.ac.cn/handle/331005/22992]  
专题上海硅酸盐研究所_特种无机涂层重点实验室_期刊论文
作者单位1.Univ Shanghai Sci & Technol, Sch Mat Sci & Engn, Shanghai 200093, Peoples R China
2.Univ Shanghai Sci & Technol, Sch Mech Engn, Shanghai 200093, Peoples R China
3.Chinese Acad Sci, Key Lab Inorgan Coating Mat, Shanghai 200050, Peoples R China
4.Changsha Univ Sci & Technol, Sch Traff & Transportat Engn, Changsha 410076, Hunan, Peoples R China
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He Daihua,Wang Pu,Liu Ping,et al. Preparation of Hydroxyapatite-titanium Dioxide Coating on Ti6Al4V Substrates using Hydrothermal-electrochemical Method[J]. JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,2016,31(2):461-467.
APA He Daihua.,Wang Pu.,Liu Ping.,Liu Xinkuan.,Ma Fengcang.,...&Ye Hong.(2016).Preparation of Hydroxyapatite-titanium Dioxide Coating on Ti6Al4V Substrates using Hydrothermal-electrochemical Method.JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,31(2),461-467.
MLA He Daihua,et al."Preparation of Hydroxyapatite-titanium Dioxide Coating on Ti6Al4V Substrates using Hydrothermal-electrochemical Method".JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION 31.2(2016):461-467.
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