Preparation of CuS with Flower-Like Morphology by Water/Ethanol Solvothermal Synthesis | |
Li, Maohua1,2,3; Hao JY(郝俊英)3; Lu, Yi1,2; Fan MJ(凡明锦)3; Yang, Bo2; Liu, Yumei1 | |
刊名 | Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry |
2016 | |
卷号 | 46期号:9页码:1415-1421 |
关键词 | copper sulfide flower-like morphology solvothermal synthesis hydrophilic |
ISSN号 | 1553-3174 |
通讯作者 | Liu, Yumei |
英文摘要 | CuS, with a flower-like morphology, has been prepared using a facile solvothermal treatment, with copper chloride (CuCl2.2H2O) and thiourea (CH4N2S) in water and dilute ethanol (water/ethanol = 1/1), at 150°C for 15 h without the assistance of a surfactant. The products were characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectroscopy, X-ray photoelectron spectroscopy, Raman spectroscopy, and UV–vis optical absorption spectroscopy. The resultant CuS flowers, with diameters ˜5 µm, were assembled by sheets. The influences of different solvent systems and varying copper sources on the CuS morphology were also investigated. The results reveal that the hydrophilicity, polarity, and viscosity of the solvent have great influences on the morphology and size of the CuS products. The possible growth mechanisms of flower-like CuS were discussed. The optical properties of the products were also recorded by means of UV-vis absorption spectroscopy. |
学科主题 | 材料科学与物理化学 |
收录类别 | SCI |
资助信息 | the National Natural Science Foundation of China (No. 51375471);the major project of Xinjiang Bureau of Quality and Technical Supervision (No. 2013-01);the Science and Technology Project of State Quality Inspection Administration (2013QK086) |
语种 | 英语 |
WOS记录号 | WOS:000382306600020 |
内容类型 | 期刊论文 |
源URL | [http://210.77.64.217/handle/362003/20687] |
专题 | 兰州化学物理研究所_固体润滑国家重点实验室 |
作者单位 | 1.Xinjiang Univ, Coll Chem & Chem Engn, Urumqi 830046, Xinjing, Peoples R China 2.Xinjiang Supervis & Inspect Inst Prod Qual, Urumqi, Xinjing, Peoples R China 3.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Solid Lubricat, Lanzhou, Peoples R China |
推荐引用方式 GB/T 7714 | Li, Maohua,Hao JY,Lu, Yi,et al. Preparation of CuS with Flower-Like Morphology by Water/Ethanol Solvothermal Synthesis[J]. Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry,2016,46(9):1415-1421. |
APA | Li, Maohua,Hao JY,Lu, Yi,Fan MJ,Yang, Bo,&Liu, Yumei.(2016).Preparation of CuS with Flower-Like Morphology by Water/Ethanol Solvothermal Synthesis.Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry,46(9),1415-1421. |
MLA | Li, Maohua,et al."Preparation of CuS with Flower-Like Morphology by Water/Ethanol Solvothermal Synthesis".Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry 46.9(2016):1415-1421. |
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