Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions

CORC > 兰州化学物理研究所 > 中国科学院兰州化学物理研究所 > OSSO国家重点实验室

	Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions
	Zhao XH(赵新红)1; Zhao, Jiangbo 1; Wen, Juanjuan 1; Li A(李安)1; Li GX(李贵贤)1; Wang XL(王晓来)2
刊名	Microporous and Mesoporous Materials
	2015
卷号	213 页码:192-196
关键词	AlPO4-5 Solvent-free Hierarchical porous Microwave
ISSN号	1387-1811
通讯作者	赵新红
英文摘要	AlPO₄-5 aluminophosphate molecular sieve with AFI topology has been successfully synthesized by microwave irradiation under solvent-free conditions. The key influential factors controlling the crystallization of AFI structure were thoroughly investigated. The optimum synthetic conditions of this material are as follows: the initial composition is 1.0Al₂O₃: 3.0P₂O₅: 2.0HF: 8.0TEABr(tetraethylammonium bromide): 125C, aluminum isopropoxide is the best aluminum source, and activated carbon needs to be pretreated before used as the reaction medium and hard template. The resultant AlPO₄-5 molecular sieves were characterized by X-ray diffraction (XRD), N₂ physisorption, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results reveal that the obtained samples exhibit hierarchically porous characteristic.
学科主题	物理化学与绿色催化
收录类别	SCI
资助信息	the National Natural Science Foundation of China (Grant No. 21306072;51263012);Development Program of Lanzhou University of Technology for excellent teachers (Grant No. Q201113)
语种	英语
WOS记录号	WOS:000356186900024
内容类型	期刊论文
源URL	[http://210.77.64.217/handle/362003/18337]
专题	兰州化学物理研究所_OSSO国家重点实验室
作者单位	1.Lanzhou Univ Technol, Sch Petrochem Engn, Lanzhou 730050, Peoples R China 2.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Oxo Synth & Select Oxidat, Lanzhou 730000, Peoples R China
推荐引用方式 GB/T 7714	Zhao XH,Zhao, Jiangbo,Wen, Juanjuan,et al. Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions[J]. Microporous and Mesoporous Materials,2015,213:192-196.
APA	Zhao XH,Zhao, Jiangbo,Wen, Juanjuan,Li A,Li GX,&Wang XL.(2015).Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions.Microporous and Mesoporous Materials,213,192-196.
MLA	Zhao XH,et al."Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions".Microporous and Mesoporous Materials 213(2015):192-196.